Making Salts
Prepare a pure, dry sample of a soluble salt from an insoluble base and an acid.
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Here you can read the aim, equipment, safety notes, examiner tips and the first few method steps. The full practical also includes the interactive simulator, mark scheme keywords, a mini quiz, exam-style practice questions and a printable revision summary.
Method
- Measure a fixed volume of the acid and pour it into a beaker.
- Warm the acid gently.
- Add the insoluble base in small masses.
- Continue adding until the base is in excess.
Aim
- Make pure, dry crystals of a soluble salt from an insoluble base and an acid.
Equipment
- Acid
- Insoluble base
- Beaker, tripod, gauze and Bunsen burner
- Filter funnel and filter paper
- Evaporating basin
- Crystallising dish
- Glass rod
Safety
- Wear eye protection because acids are irritants.
- Use gentle heating and keep the Bunsen flame controlled.
- Handle hot glassware with care.
Common mistakes
- Adding too little base so acid remains in the final solution.
- Forgetting that copper sulfate is soluble and passes through the filter.
- Writing evaporate all the water instead of crystallise the solution.
Examiner tips
Examiner insight
Use the word excess to explain why all acid is neutralised.
Examiner insight
Filtration removes the insoluble reactant, not the dissolved salt.
Examiner insight
Evaporate to the point of crystallisation rather than boiling to dryness.
Variables
- Independent
- Mass of base added, or type of acid/base depending on investigation.
- Dependent
- Mass and quality of salt crystals produced.
- Control
- Volume and concentration of acid, Temperature, Evaporation time, Cooling conditions
Working scientifically
- Accuracy
- How close the mass of crystals obtained is to the mass predicted from the reacting masses.
- Precision
- How similar the masses of crystals are if the practical is repeated using the same method.
- Reliability
- Whether repeating the preparation gives a similar yield and appearance of crystals each time.
- Validity
- Whether all of the acid has actually reacted, so the crystals collected are a pure sample of the salt.
Common exam questions
- Why is excess base added?
- Why is the mixture filtered?
- Why should the solution not be heated to dryness?
Continue with the full practical
The full version includes the interactive simulator, mini quiz feedback, exam-style practice questions with model answers, saved notes and a print-friendly revision summary.